By Lionel M. Levinson, Shin-Ichi Hirano
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Extra resources for Grain boundaries and interfacial phenomena in electronic ceramics
15 M, reaction (1) was very fast and no morphological evolution of precipitate particles could be observed on the time scale considered. Powders were composed of crystalline(cubic simmetry) spherical particles with average size in the range of 30-50 nm. 31 M and aged 100 h is presented in figure 1. Figure 1. 31 M and aged for 100 h. On the contrary, when [Ba2+]owas reduced, a certain amount of amorphous phase was present as indicated by a broad contribution to XRD profiles between 20 and 50" 28.
Levi, “Low Temperature/Low Pressure Hydrothermal Synthesis of Barium Titanate: Powder and heteroepitaxial Thin Films,” J. Mater. , 10  1784-89 (1995). ’R. Vivekanandan and T. R. N. , 57 181-92 (1989). ‘OM. H. Frey and D. A. Payne, “Grain Size Efeects on Structure and Phase Transformations for Barium Titanate,” Phys. , 54 [ 5 ] 3 158-68 (1996). ‘D. Hennings and S. Schreinemacher, “Characterization of Hydrothermal Barium Titanate,”J. Europ. Ceram. , 9 41-46 (1992). D. Begg, E. R. Vance, and J.
E. before spontaneous crystallisation of BaTi03. 0 __ 45 0 Figure 3. 25 hours. l=BaTi03, 2=BaTi205,3=Ba4Ti13030. On the contrary, BaTi03 was detected after thermal treatment when it was already present as a crystalline phase in the as-prepared powder. Therefore, it can be assumed that the treatment applied wasn’t sufficient to reach equilibrium but only to transform the amorphous phase. Results of Rietveld calculations are plotted in Figure 4 together with specific surface area (SBET) data measured on the same samples.
Grain boundaries and interfacial phenomena in electronic ceramics by Lionel M. Levinson, Shin-Ichi Hirano